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J Adv Prosthodont 2015;7:85-92
http://dx.doi.org/10.4047/jap.2015.7.2.85
Efficacy of various cleaning solutions on saliva-contaminated zirconia for improved resin bonding Da-Hye Kim1, Jun-Sik Son2, Seong-Hwa Jeong3, Young-Kyung Kim4, Kyo-Han Kim5, Tae-Yub Kwon5* Department of Medical & Biological Engineering, Graduate School, Kyungpook National University, Daegu, Republic of Korea Korea Textile Development Institute, Daegu, Republic of Korea 3 Faculty of Health Science, Daegu Haany University, Gyeongsan, Republic of Korea 4 Department of Conservative Dentistry, School of Dentistry, Kyungpook National University, Daegu, Republic of Korea 5 Department of Dental Biomaterials, School of Dentistry, Kyungpook National University, Daegu, Republic of Korea 1 2
PURPOSE. This study aimed to investigate the efficacy of cleaning solutions on saliva-contaminated zirconia in comparison to air-abrasion in terms of resin bonding. MATERIALS AND METHODS. For saliva-contaminated airabraded zirconia, seven cleaning methods)–no contamination (NC), water-spray rinsing (WS), additional airabrasion (AA), and cleaning with four solutions (Ivoclean [IC]; 1.0 wt% sodium dodecyl sulfate [SDS], 1.0 wt% hydrogen peroxide [HP], and 1.0 wt% sodium hypochlorite [SHC])–were tested. The zirconia surfaces for each group were characterized using various analytical techniques. Three bonded resin (Panavia F 2.0) cylinders (bonding area: 4.5 mm2) were made on one zirconia disk specimen using the Ultradent jig method [four disks (12 cylinders)/group; a total of 28 disks]. After 5,000 thermocycling, all specimens were subjected to a shear bond strength test with a crosshead speed of 1.0 mm/minute. The fractured surfaces were observed using an optical and scanning electron microscope (SEM). RESULTS. Contact angle measurements showed that groups NC, AA, IC, and SHC had hydrophilic surfaces. The X-ray photoelectron spectroscopy (XPS) analysis showed similar elemental distributions between group AA and groups IC and SHC. Groups IC and SHC showed statistically similar bond strengths to groups NC and AA (P>.05), but not groups SDS and HP (P.999
J Adv Prosthodont 2015;7:85-92
http://dx.doi.org/10.4047/jap.2015.7.2.85
Efficacy of various cleaning solutions on saliva-contaminated zirconia for improved resin bonding Da-Hye Kim1, Jun-Sik Son2, Seong-Hwa Jeong3, Young-Kyung Kim4, Kyo-Han Kim5, Tae-Yub Kwon5* Department of Medical & Biological Engineering, Graduate School, Kyungpook National University, Daegu, Republic of Korea Korea Textile Development Institute, Daegu, Republic of Korea 3 Faculty of Health Science, Daegu Haany University, Gyeongsan, Republic of Korea 4 Department of Conservative Dentistry, School of Dentistry, Kyungpook National University, Daegu, Republic of Korea 5 Department of Dental Biomaterials, School of Dentistry, Kyungpook National University, Daegu, Republic of Korea 1 2
PURPOSE. This study aimed to investigate the efficacy of cleaning solutions on saliva-contaminated zirconia in comparison to air-abrasion in terms of resin bonding. MATERIALS AND METHODS. For saliva-contaminated airabraded zirconia, seven cleaning methods)–no contamination (NC), water-spray rinsing (WS), additional airabrasion (AA), and cleaning with four solutions (Ivoclean [IC]; 1.0 wt% sodium dodecyl sulfate [SDS], 1.0 wt% hydrogen peroxide [HP], and 1.0 wt% sodium hypochlorite [SHC])–were tested. The zirconia surfaces for each group were characterized using various analytical techniques. Three bonded resin (Panavia F 2.0) cylinders (bonding area: 4.5 mm2) were made on one zirconia disk specimen using the Ultradent jig method [four disks (12 cylinders)/group; a total of 28 disks]. After 5,000 thermocycling, all specimens were subjected to a shear bond strength test with a crosshead speed of 1.0 mm/minute. The fractured surfaces were observed using an optical and scanning electron microscope (SEM). RESULTS. Contact angle measurements showed that groups NC, AA, IC, and SHC had hydrophilic surfaces. The X-ray photoelectron spectroscopy (XPS) analysis showed similar elemental distributions between group AA and groups IC and SHC. Groups IC and SHC showed statistically similar bond strengths to groups NC and AA (P>.05), but not groups SDS and HP (P.999
